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High-Resolution NMR Techniques in Organic Chemistry Vital Source e-bog
Timothy D.W. Claridge
(2016)
High-Resolution NMR Techniques in Organic Chemistry
Timothy D. W. Claridge
(2016)
Sprog: Engelsk
Detaljer om varen
- 3. Udgave
- Vital Source searchable e-book (Reflowable pages): 552 sider
- Udgiver: Elsevier Science (April 2016)
- ISBN: 9780080999937
High-Resolution NMR Techniques in Organic Chemistry, Third Edition, describes the most important NMR spectroscopy techniques for structure elucidation of organic molecules and the investigation of their behavior in solution. Appropriate for students as well as chemists, this thorough revision covers the practical aspects of NMR instrumentation and explores the capabilities and the limitations of key one-dimensional and two-dimensional analytical methods including J-resolved, nuclear Overhauser, diffusion, and experimental spectroscopic techniques.
The Third Edition includes valuable updates on recent hardware developments and common and novel techniques. It also features an entirely new chapter on using NMR methods to study protein-ligand binding processes, reflecting this area’s growing importance for life science and medicinal chemistry research in industry and academia. Using accessible figures to present and explain techniques, the book limits complex mathematical descriptions and provides multiple worked examples throughout. Additionally, a new, cumulative "Example Problem Solving" chapter demonstrates the application of described methods with readily available samples; readers can view the spectra, follow the interpretation, and collect their own data for comparison and practice.
A trusted authority on this critical expertise, High-Resolution NMR Techniques in Organic Chemistry, Third Edition, is an essential resource for every NMR manager and chemistry student.
- Uniquely covers both the hardware and the analysis of NMR techniques
- Includes valuable updates on the important, growing area of Ligand-protein binding, recent hardware developments, and additional practical examples
- Focuses on methods and examples vital for the practicing and student chemist
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Detaljer om varen
- Paperback: 552 sider
- Udgiver: Elsevier Science & Technology (Maj 2016)
- ISBN: 9780080999869
High-Resolution NMR Techniques in Organic Chemistry, Third Edition describes the most important NMR spectroscopy techniques for the structure elucidation of organic molecules and the investigation of their behaviour in solution. Appropriate for advanced undergraduate and graduate students, research chemists and NMR facility managers, this thorough revision covers practical aspects of NMR techniques and instrumentation, data collection, and spectrum interpretation. It describes all major classes of one- and two-dimensional NMR experiments including homonuclear and heteronuclear correlations, the nuclear Overhauser effect, diffusion measurements, and techniques for studying protein-ligand interactions. A trusted authority on this critical expertise, High-Resolution NMR Techniques in Organic Chemistry, Third Edition is an essential resource for every chemist and NMR spectroscopist.
2. Introducing High-Resolution NMR
3. Practical Aspects of High-Resolution NMR
4. One-Dimensional Techniques
5. Introducing Two-Dimensional and Pulsed Field Gradient NMR
6. Correlations Through the Chemical Bond I: Homonuclear Shift Correlation
7. Correlations Through the Chemical Bond II: Heteronuclear Shift Correlation
8. Separating Shifts and Couplings: J-Resolved and Pure Shift Spectroscopy
9. Correlations Through Space: The Nuclear Overhauser Effect
10. Diffusion NMR Spectroscopy
11. Protein-Ligand Screening by NMR
12. Experimental Methods
13. Structure Elucidation and Spectrum Assignment