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A Microscale Approach to Organic Laboratory Techniques Vital Source e-bog
Donald L. Pavia
(2017)
Cengage Learning
699,00 kr.
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A Microscale Approach to Organic Laboratory Techniques
Donald L. Pavia, George S. Kriz, Gary M. Lampman og Randall G. Engel
(2017)
Sprog: Engelsk
Brooks/Cole
1.210,00 kr.
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Detaljer om varen
- 6. Udgave
- Vital Source searchable e-book (Fixed pages)
- Udgiver: Cengage Learning (Januar 2017)
- ISBN: 9781337516280
Taking an organic chemistry laboratory course? You need a laboratory textbook you can trust! This proven book gives you what you need to conduct a variety of interesting microscale experiments with safety and ease -- while you develop an understanding of the special techniques these types of experiments require.
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Bookshelf online: 5 år fra købsdato.
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Print: 2 sider kan printes ad gangen
Copy: højest 2 sider i alt kan kopieres (copy/paste)
Bookshelf online: 5 år fra købsdato.
Bookshelf appen: ubegrænset dage fra købsdato.
Udgiveren oplyser at følgende begrænsninger er gældende for dette produkt:
Print: 2 sider kan printes ad gangen
Copy: højest 2 sider i alt kan kopieres (copy/paste)
Detaljer om varen
- 6. Udgave
- Hardback: 1056 sider
- Udgiver: Brooks/Cole (Januar 2017)
- Forfattere: Donald L. Pavia, George S. Kriz, Gary M. Lampman og Randall G. Engel
- ISBN: 9781305968349
Taking an organic chemistry laboratory course? You need a laboratory textbook you can trust! This proven book gives you what you need to conduct a variety of interesting microscale experiments with safety and ease -- while you develop an understanding of the special techniques these types of experiments require.
Experiment
1.Introduction to Microscale Laboratory.Experiment
2.Solubility.Experiment
3.Crystallization.Experiment
4.Extraction.Experiment
5.A Separation and Purification Scheme.Experiment
6.Chromatography.Experiment
7.Infrared Spectroscopy and Boiling Point Determination.Experiment
8.Simple and Fractional Distillation.Essay: Aspirin.Experiment
9.Acetylsalicylic Acid.Essay: Analgesics.Experiment
10. Isolation of the Active Ingredient in an Analgesic Drug.Experiment 11, Acetaminophen.Essay: Identification of Drugs.Experiment
12. TLC Analysis of Analgesic Drugs.Essay: Caffeine.Experiment
13. Isolation of Caffeine from Tea or Coffee.Essay: Esters -- Flavors and Fragrances.Experiment
14. Isopentyl Acetate (Banana Oil).Essay: Terpenes and Phenylpropanoids.Experiment
15. Essential Oils: Extraction of Oil of Cloves by Steam Distillation.Essay: Stereochemical Theory of Odor.Experiment
16. Spearmint and Caraway Oil: (+)- and (-)-Carvones.Essay: The Chemistry of Vision.Experiment
17. Isolation of Chlorophyll and Carotenoid Pigments from Spinach.Essay: Ethanol and Fermentation Chemistry.Experiment
18. Ethanol from Sucrose.Essay Molecular Modeling and Molecular Mechanics.Experiment
19. An Introduction to Molecular Modeling.Essay: Computational Chemistry -- Ab Initio and Semiempirical Methods.Experiment
20. Computational Chemistry.Experiment
21. Reactivities of Some Alkyl Halides.Experiment
22. Nucleophilic Substitution Reactions: Competing Nucleophiles.Experiment
23. Synthesis of n-Butyl Bromide and t-Pentyl Chloride.Experiment
24. 4-Methylcyclohexene.Essay: Fats and Oils.Experiment
25. Methyl Stearate from Methyl Oleate.Essay: Soap.Experiment
26. Preparation of Soap.Essay: Petroleum and Fossil Fuels.Experiment
27. Gas Chromatographic Analysis of Gasolines.Essay: Biofuels.Experiment
28. Biodiesel.Essay: Green Chemistry.Experiment
29. Chiral Reduction of Ethyl Acetoacetate; Optical Purity Determination.Experiment
30. Nitration of Aromatic Compounds Using a Recyclable Catalyst.Experiment
31. Reduction of Ketones Using Carrots as Biological Reducing Agents.Experiment
32. Resolution of Phenylethylamine and Determination of Optical Purity.Experiment
33. An Oxidation-Reduction Scheme: Borneol, Camphor, Isoborneol.Experiment
34. Multi-Step Reaction Sequences: The Conversion of Benzaldehydeto Benzilic Acid.Experiment
35. Triphenylmethanol and Benzoic Acid.Experiment
36. Aqueous-based Organozinc Reactions.Experiment
37. Sonogashira Coupling of Iodosubstituted Aromatic Compounds with Alkynes Using a Palladium Catalyst.Experiment
38. Grubbs-Catalyzed Metathesis of Eugenol with 1,4-Butanediol to Prepare a Natural Product.Experiment
39. The Aldol Condensation Reaction: Preparation of Benzalacetophenones (Chalcones).Experiment
40. A Green Enantioselective Aldol Condensation Reaction.Experiment
41. Preparation of an Unsaturated Ketone via Michael and Aldol Condensation Reactions.Experiment
42. Preparation of Triphenylpyridine.Experiment
43. The Wittig Reaction: Preparation of 1,4-Diphenyl-1,3-Butadiene.Experiment
44. Relative Reactivities of Several Aromatic Compounds.Experiment
45. Nitration of Methyl Benzoate.Essay: Synthetic Dyes.Experiment
46. Preparation of Methyl Orange.Experiment
47. Preparation of Indigo.Experiment
48. Formulation of a Paint and Art Project.Essay: Local Anesthetics.Experiment
49. Benzocaine.Essay: Pheromones: Insect Attractants and Repellents.Experiment
50. N,N-Diethyl-m-toluamide: The Insect Repellent OFF".Essay: Sulfa Drugs.Experiment
51. Sulfa Drugs: Preparation of Sulfanilamide.Essay: Polymers and Plastics.Experiment
52. Preparation and Properties of Polymers: Polyester, Nylon, and Polystyrene.Essay: Diels-Alder Reactions and Insecticides.Experiment
53. The Diels-Alder Reaction of Cyclopentadiene with Maleic Anhydride.Experiment
54. The Diels-Alder Reaction with Anthracene-9-Methanol.Experiment
55. Photoreduction of Benzophenone and Rearrangement of Benzpinacol to Benzopinacolone.Essay: Fireflies and Photochemistry.Experiment
56. Luminol.Experiment
57. Identification of Unknowns.Experiment
58. Preparation of a C-4 or C-5 Acetate Ester.Experiment
59. Competing Nucleophiles in SN1 and SN2 Reactions: Investigations Using 2-Pentanol and 3-Pentanol.Experiment
60. Friedel-Crafts Acylation.Experiment
61. The Analysis of Antihistamine Drugs by Gas Chromatography-Mass Spectrometry.Experiment
62. The Use of Organozinc Reagents in Synthesis: An Exercise in Synthesis and Structure Proof by Spectroscopy.Experiment
63. Synthesis of Naproxen by Palladium Catalysis.Experiment
64. The Aldehyde Enigma.Experiment
65. Synthesis of Substituted Chalcones: A Guided-Inquiry Experience.Experiment
66. Green Epoxidation of Chalcones.Experiment
67. Cyclopropanation of Chalcones.Experiment
68. Michael and Aldol Condensation Reactions.Experiment
69. Esterification Reactions of Vanillin: The Use of NMR to Solve a Structure Proof Problem. Technique
1. Laboratory Safety.Technique
2. The Laboratory Notebook, Calculations, and Laboratory Records.Technique
3. Laboratory Glassware: Care and Cleaning.Technique
4. How to Find Data for Compounds: Handbooks and Catalogs.Technique
5. Measurement of Volume and Weight.Technique
6. Heating and Cooling Methods.Technique
7. Reaction Methods.Technique
8. Filtration.Technique
9. Physical Constants of Solids: The Melting Point.Technique
10. Solubility.Technique
11. Crystallization: Purification of Solids.Technique
12. Extractions, Separations, and Drying Agents.Technique
13. Physical Constants of Liquids: The Boiling Point and Density.Technique
14. Simple Distillation.Technique
15. Fractional Distillation, Azeotropes.Technique
16. Vacuum Distillation, Manometers.Technique
17. Sublimation.Technique
18. Steam Distillation.Technique
19. Column Chromatography.Technique
20. Thin-Layer Chromatography.Technique
21. High-Performance Liquid Chromatography (HPLC).Technique
22. Gas Chromatography.Technique
23. Polarimetry.Technique
24. Refractometry.Technique
25. Infrared Spectroscopy.Technique
26. Nuclear Magnetic Resonance Spectroscopy.Technique
27. Carbon-13 Nuclear Magnetic Resonance Spectroscopy.Technique
28. Mass Spectrometry.Technique
29. Guide to the Chemical Literature.Appendix
1: Tables of Unknowns and Derivatives.Appendix
2: Procedures for Preparing Derivatives.Appendix
3: Index of Spectra.Index."
1.Introduction to Microscale Laboratory.Experiment
2.Solubility.Experiment
3.Crystallization.Experiment
4.Extraction.Experiment
5.A Separation and Purification Scheme.Experiment
6.Chromatography.Experiment
7.Infrared Spectroscopy and Boiling Point Determination.Experiment
8.Simple and Fractional Distillation.Essay: Aspirin.Experiment
9.Acetylsalicylic Acid.Essay: Analgesics.Experiment
10. Isolation of the Active Ingredient in an Analgesic Drug.Experiment 11, Acetaminophen.Essay: Identification of Drugs.Experiment
12. TLC Analysis of Analgesic Drugs.Essay: Caffeine.Experiment
13. Isolation of Caffeine from Tea or Coffee.Essay: Esters -- Flavors and Fragrances.Experiment
14. Isopentyl Acetate (Banana Oil).Essay: Terpenes and Phenylpropanoids.Experiment
15. Essential Oils: Extraction of Oil of Cloves by Steam Distillation.Essay: Stereochemical Theory of Odor.Experiment
16. Spearmint and Caraway Oil: (+)- and (-)-Carvones.Essay: The Chemistry of Vision.Experiment
17. Isolation of Chlorophyll and Carotenoid Pigments from Spinach.Essay: Ethanol and Fermentation Chemistry.Experiment
18. Ethanol from Sucrose.Essay Molecular Modeling and Molecular Mechanics.Experiment
19. An Introduction to Molecular Modeling.Essay: Computational Chemistry -- Ab Initio and Semiempirical Methods.Experiment
20. Computational Chemistry.Experiment
21. Reactivities of Some Alkyl Halides.Experiment
22. Nucleophilic Substitution Reactions: Competing Nucleophiles.Experiment
23. Synthesis of n-Butyl Bromide and t-Pentyl Chloride.Experiment
24. 4-Methylcyclohexene.Essay: Fats and Oils.Experiment
25. Methyl Stearate from Methyl Oleate.Essay: Soap.Experiment
26. Preparation of Soap.Essay: Petroleum and Fossil Fuels.Experiment
27. Gas Chromatographic Analysis of Gasolines.Essay: Biofuels.Experiment
28. Biodiesel.Essay: Green Chemistry.Experiment
29. Chiral Reduction of Ethyl Acetoacetate; Optical Purity Determination.Experiment
30. Nitration of Aromatic Compounds Using a Recyclable Catalyst.Experiment
31. Reduction of Ketones Using Carrots as Biological Reducing Agents.Experiment
32. Resolution of Phenylethylamine and Determination of Optical Purity.Experiment
33. An Oxidation-Reduction Scheme: Borneol, Camphor, Isoborneol.Experiment
34. Multi-Step Reaction Sequences: The Conversion of Benzaldehydeto Benzilic Acid.Experiment
35. Triphenylmethanol and Benzoic Acid.Experiment
36. Aqueous-based Organozinc Reactions.Experiment
37. Sonogashira Coupling of Iodosubstituted Aromatic Compounds with Alkynes Using a Palladium Catalyst.Experiment
38. Grubbs-Catalyzed Metathesis of Eugenol with 1,4-Butanediol to Prepare a Natural Product.Experiment
39. The Aldol Condensation Reaction: Preparation of Benzalacetophenones (Chalcones).Experiment
40. A Green Enantioselective Aldol Condensation Reaction.Experiment
41. Preparation of an Unsaturated Ketone via Michael and Aldol Condensation Reactions.Experiment
42. Preparation of Triphenylpyridine.Experiment
43. The Wittig Reaction: Preparation of 1,4-Diphenyl-1,3-Butadiene.Experiment
44. Relative Reactivities of Several Aromatic Compounds.Experiment
45. Nitration of Methyl Benzoate.Essay: Synthetic Dyes.Experiment
46. Preparation of Methyl Orange.Experiment
47. Preparation of Indigo.Experiment
48. Formulation of a Paint and Art Project.Essay: Local Anesthetics.Experiment
49. Benzocaine.Essay: Pheromones: Insect Attractants and Repellents.Experiment
50. N,N-Diethyl-m-toluamide: The Insect Repellent OFF".Essay: Sulfa Drugs.Experiment
51. Sulfa Drugs: Preparation of Sulfanilamide.Essay: Polymers and Plastics.Experiment
52. Preparation and Properties of Polymers: Polyester, Nylon, and Polystyrene.Essay: Diels-Alder Reactions and Insecticides.Experiment
53. The Diels-Alder Reaction of Cyclopentadiene with Maleic Anhydride.Experiment
54. The Diels-Alder Reaction with Anthracene-9-Methanol.Experiment
55. Photoreduction of Benzophenone and Rearrangement of Benzpinacol to Benzopinacolone.Essay: Fireflies and Photochemistry.Experiment
56. Luminol.Experiment
57. Identification of Unknowns.Experiment
58. Preparation of a C-4 or C-5 Acetate Ester.Experiment
59. Competing Nucleophiles in SN1 and SN2 Reactions: Investigations Using 2-Pentanol and 3-Pentanol.Experiment
60. Friedel-Crafts Acylation.Experiment
61. The Analysis of Antihistamine Drugs by Gas Chromatography-Mass Spectrometry.Experiment
62. The Use of Organozinc Reagents in Synthesis: An Exercise in Synthesis and Structure Proof by Spectroscopy.Experiment
63. Synthesis of Naproxen by Palladium Catalysis.Experiment
64. The Aldehyde Enigma.Experiment
65. Synthesis of Substituted Chalcones: A Guided-Inquiry Experience.Experiment
66. Green Epoxidation of Chalcones.Experiment
67. Cyclopropanation of Chalcones.Experiment
68. Michael and Aldol Condensation Reactions.Experiment
69. Esterification Reactions of Vanillin: The Use of NMR to Solve a Structure Proof Problem. Technique
1. Laboratory Safety.Technique
2. The Laboratory Notebook, Calculations, and Laboratory Records.Technique
3. Laboratory Glassware: Care and Cleaning.Technique
4. How to Find Data for Compounds: Handbooks and Catalogs.Technique
5. Measurement of Volume and Weight.Technique
6. Heating and Cooling Methods.Technique
7. Reaction Methods.Technique
8. Filtration.Technique
9. Physical Constants of Solids: The Melting Point.Technique
10. Solubility.Technique
11. Crystallization: Purification of Solids.Technique
12. Extractions, Separations, and Drying Agents.Technique
13. Physical Constants of Liquids: The Boiling Point and Density.Technique
14. Simple Distillation.Technique
15. Fractional Distillation, Azeotropes.Technique
16. Vacuum Distillation, Manometers.Technique
17. Sublimation.Technique
18. Steam Distillation.Technique
19. Column Chromatography.Technique
20. Thin-Layer Chromatography.Technique
21. High-Performance Liquid Chromatography (HPLC).Technique
22. Gas Chromatography.Technique
23. Polarimetry.Technique
24. Refractometry.Technique
25. Infrared Spectroscopy.Technique
26. Nuclear Magnetic Resonance Spectroscopy.Technique
27. Carbon-13 Nuclear Magnetic Resonance Spectroscopy.Technique
28. Mass Spectrometry.Technique
29. Guide to the Chemical Literature.Appendix
1: Tables of Unknowns and Derivatives.Appendix
2: Procedures for Preparing Derivatives.Appendix
3: Index of Spectra.Index."
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